Parr-instrument 1356 Instrukcja Użytkownika

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No. 434M
1356 ISOPERIBOL BOMB CALORIMETER
Service Manual
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1 2 3 4 5 6 ... 40 41

Podsumowanie treści

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No. 434M 1356 ISOPERIBOL BOMB CA

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10 nitrogen that was present as part of the air trapped in the bomb is burned to nitric oxide which combines with water vapor to form nitric a

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11 Spiking Calculations [{EE x T(temp rise)}-e1-e2-e3-[mass(oil) x Heat Combustion(oil)]/sample m grams 2. 1108 Oxygen Bomb Maintenance and Safe

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12 Sample preparation

Strona 5 - 1. Calorimeter Operation

13 the 238A sealing ring ages and hardens it becomes a partial electrical conductor, permitting misfires and producing unwanted heating effects.

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14 2. Parts Replacement Keyboard A bad keyboard panel will result in the calorimeter responding to only some rows or columns of keys and ignor

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15 the left side panel via velcro and is located between the power supply board at the front and the cpu board and is connected electrically to th

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16 4. Remove the six screws located on the display bezel and remove the bezel. 5. Push the rear of the controller near the bottom of the cas

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17 12. Position the new mounting plates on the shaft assembly rod. Raise the shaft assembly rod to position the support rod mounting plate ove

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188. Misfire Error Ignition Problems on the 1356 Calorimeter are generally attributed to one of three possible sources, after having checked

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19 Low Oxygen Charge Low Oxygen Pressure - signifies low oxygen pressure in the line filling the bomb. The

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20 Oxygen Use P1A Oxygen Cylinder volume of cylinder 43.8 liters pressure of cylinder 2490 psi V x P = 109062 liters-psi Amount of gas

Strona 14 - 2. Parts Replacement

21 1. Solid Fuels (D2015) Heat of Formation of ... 29KJ/mole Sulfuric Acid for a Fuel with 5% sulfur and 5% hydrogen S02(g) + 1/2 02(g) + H20(1

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22 4. Nitrogen 1.251 gm x 10.8 liter = 13.51 gm .249 cal x 13.51 gm = 3.36 cal gm K K oxygen 3.4 cal/C argon 2.4

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231356 Data Logger To log data one may either log the data to the internal ram disc, or send the data directly to the printer or to the computer.

Strona 17 - 4. Messages Error

24 The 1356 Calorimeter Controller can be physically separated into two halves. The upper part consists of the keyboard, LCD display, keypad and disp

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25 Lengthening Post Period for 1356 Calorimeter Gain entry to the factory menu by pressing the following three keys simultaneously from the main m

Strona 19 - 5. Miscellaneous

26 attached to the display. Set the display to the side. Care should be taken to avoid scratching the display. 4. Remove the 5 screws holding

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27 1356 Calorimeter Parts List Item Description Item Description 421A A476A3 393DD 1027DD 539DD 549DD 558DD

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28 Recommended Spare Parts Per 5000 Tests Qty. Part No. Description 3 PKG (2) 3 PKG (2) 1 PKG (12) 3 PKG (12) 1 PKG (2) 1 PKG (2) 1 3 PKG (2)

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29 Parts Hinge Assembly Qty Part No Description 1 A525DD Lower RH Link 1 A526DD Lower LH Link 2 527DD Li

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1. Calorimeter Operation Operation……………………………………………………………………5 Corrections Fixed………………………………………………………… 6 Corr

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30 Parts List 1563 Water Handling System Part No. Description 108C 110C 148C 149C 186DD 612DD A633DDEA A633DDEF 894DD 34E2 138E 178E 185E 20

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31 1356 Calorimeter Front View SA1332RD06Lower L

Strona 27 - 1356 Calorimeter Parts List

33 A546DD2 Left Bracket Linkage

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34 A535DD3 Right Mounting Plate

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35 A545DD2 Right Bracket Link

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36 1356 Cover Assembly Assembly

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Diagram Flow

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Electrical Diagrams Water Handling

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39 MSDS-Benzoic Acid ----------------------------------------------------------------------- 1 - PRODUCT IDENTIFICATION ------------------------

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4 MSDS sheet benzoic acid…………………………………………………. 41

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40 FIRE EXTINGUISHING MEDIA USE ALCOHOL FOAM, DRY CHEMICAL OR CARBON DIOXIDE. (WATER MAY BE INEFFECTIVE.) SPECIAL FIRE-FIGHTING PROCEDURES FIR

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41----------------------------------------------------------------------- 7 - SPILL AND DISPOSAL PROCEDURES --------------------------------------

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5 1. Calorimeter Operation A. Operating the Calorimeter

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6 Press the START key . The calorimeter will prompt for a Cal ID. The calorimeter will then prompt for sam

Strona 39 - MSDS-Benzoic Acid

7 B. Entering Corrections and Obtaining the Final Report Final reports for each test can be obtained via the REPORT key, whenever the user is pr

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8 Reports may be obtained by pressing the REPORT key. To obtain a block of reports between two specified sample numbers, press the REPORT key.

Strona 41 - Revision 2-20-03

9 Press the Clear key, enter the new value on the keyboard and press the Enter key. This sequence is canceled by pressing the RESET key. Press

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